Operation of the Balance
Micro, semi-micro, analytical and precision balances are measuring
instruments of the highest precision. The following points will help you
obtain reliable weighing results.
Switching on
Do not disconnect the balance from the power
supply and always leave it switched on. This allows the balance to
reach thermal equilibrium.
- When you switch the balance off, use the display key (on older
models the tare key). The balance is now in standby mode. The
electronics are still energized and no warm-up period is
necessary.
TIP: We recommend a different warm-up time for
each balance when it is first connect to the power supply. These
are:
- Up to 12 hours for micro balances
- Approximately 6 hours for semi-micro and analytical balances
- Approximately 3 hours for precision balances
Apart from these guidelines, always observe the minimum times
specified in the operating instructions.
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Leveling
Align the balance. To do this, check that
the air bubble is in the center of the level indicator. Use the
leveling feet to make adjustments. You must then adjust the sensitivity
of the balance. The exact procedure is described in the operating
instructions for the balance.
TIP: To ensure and document that the balance
is correctly leveled every time for example, to comply with
GxP1) we recommend the Excellence Plus family of balances
with the built-in automatic warning function “LevelControl”.
1) GxP Good Laboratory Practice (GLP) or Good
Manufacturing Practice (GMP)
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Adjustment
Adjust the sensitivity of the balance
regularly, especially
- when you operate the balance for the first time
- when you change the location of the balance
- after leveling the balance
- after major changes in temperature, humidity or air pressure.
TIP: If a fully automatic calibration
following, for example, a temperature change is important to you, it
would be worthwhile to acquire balances with “FACT,” which calibrate
automatically. These models also allow you to extend the time interval
for routine checks.
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Reading
Check that the balance displays exactly zero
at the start of each weighing. Tare, if needed, to avoid zero
errors.
- Read off the result only after the small round circle in the upper
left of the balance display has faded. The weighing result is released
through this stability detector.
TIP: The Excellence Plus line offers an
advanced stability detector. These balances display unstable
measurement values in blue. Once stability is regained, the
display immediately changes to black and the circle in the upper
left disappears. This allows you to identify a stable weighing result
faster, safer and more reliably.
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Weighing pan
Always place the weighing sample in the
middle of the weighing pan. This will prevent corner load errors.
- With micro and semi-micro balances, the weighing pan should first
be loaded once briefly after a relatively long pause (>30 min) to
deactivate the “initial weighing effect”.
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Weighing vessel
Use the smallest
possible weighing vessel.
- Avoid weighing vessels made of plastic when atmospheric humidity is
below 30-40 %. These conditions increase the risk of electrostatic
charge.
Materials with a high degree of electrical insulation, such as glass
and plastic, can become electrostatically charged. This can drastically
distort the weighing result. For this reason, make sure you take the
appropriate corrective measures (for more, see
Electrostatics)
- The weighing vessel and the sample it contains should have the same
temperature as the surroundings. Temperature differences can lead to
aircurrents that distort the weighing result (see Temperature). After
removing the weighing vessel from a drying oven or dishwasher, allow it
time to cool before placing it on the balance.
- If possible, do not use your hands to place the weighing vessel in
the weighing chamber. You could alter the temperature and atmospheric
humidity of the weighing chamber and the weighing vessel, which would
have an adverse effect on the measurement process.
 TIP: Different taring
container holders offer optimal conditions for error-free and safe
weighing (see illustrations).
Round bottomed flasks on special taring
container holders “ErgoClip Flask” and “MinWeigh Door”.
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Draft shield
Open the draft shield only as far as
necessary. This will keep the climate in the weighing chamber constant,
and the weighing result will not be influenced.
- Adjust balances that have an automatic and configurable draft
shield, such as the instruments of the Excellence Plus family, so that
the opening of the draft shield is minimal.
TIP: To make weighing simpler and more
precise, even under the most challenging conditions, we recommend
specific accessories for our Excellence and Excellence Plus families of
balances. These balances will yield the best results, even when you are
weighing extremely small samples with narrow tolerances under
unfavorable ambient conditions. Our special draft shield “MinWeigh
Door,” for example, is designed to be perfect for use in weighing
cabinets. But it also offers advantages for “normal” weighing
conditions. It can improve the repeatability of the net reading by a
factor of about two!
Using “SmartGrid,” a weighing pan with a special grid structure,
stabilizes weighing so well that the draft shield doors for 4-digit
analytical balances can normally be left open during weighing.
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Care of the balance
Keep the weighing chamber and weighing pan
clean.
- Use only clean vessels for weighing.
- The balance can be cleaned with conventional window-cleaning
fluid.
- Do not use cloths that contain fusel oil.
- Do not brush contaminants into potential openings.
- Before cleaning, remove all removable parts, such as the weighing
pan.
TIP: On Excellence and Excellence Plus
analytical balances, each of the draft shield panes can be removed for
cleaning in a dishwasher.
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